Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC2N Ceramic
نویسندگان
چکیده
Bulk B-C-N materials were synthesized under static high thermobaric conditions (20 GPa and 2,000 °C) in a multianvil apparatus from a polymer derived t-BC1.97N ceramic. The bulk samples were characterised using X-ray synchrotron radiation and analytical transmission electron microscopy in combination with electron energy loss spectroscopy. Polycrystalline B-C-N materials with a cubic type structure were formed under the applied reaction conditions, but the formation of a ternary cubic diamond-like c-BC2N compound, could not be unambiguously confirmed. OPEN ACCESS Materials 2011, 4 2062
منابع مشابه
Synthesis and characterization of high-temperature ceramic YBCO nanostructures prepared from a novel precursor
As a new precursor, [tris(2-hydroxyacetophenato) triaqua(III)], [Y(HAP)3(H2O)3]; complex was used in thermal decomposition process for the synthesis of rod-like high-temperature ceramic YBCO with length of about 320-350 nm and diameters 60–90 nm. The as-synthesized products were characterized by XRD, FT-IR, TEM, SEM and EDX analyses. The results showed that by u...
متن کاملSynthesis of cyclic olefin polymers with high glass transition temperature and high transparency using tungsten-based catalyst system
Novel cyclic olefin polymers (COPs) derived from bulky cyclic olefins, tricyclodipentadiene (TCPD) and tricyclo[6.4.0.19,12]-tridec-10-ene (TTE), with high glass transition temperature (Tg), excellent thermal stability, and high transparency, have been synthesized by ring-opening metathesis polymerization (ROMP) and subsequent hydrogenation. ROMP of TCPD and TTE was carried out successfully wit...
متن کاملEnhancing the bioactivity of a calcium phosphate glass-ceramic with controlled heat treatment
In this paper synthesis and characterization of a bioactive calcium phosphate glass-ceramic is presented, synthesized using a facile method. The glass-ceramic samples are synthesized with heat treating the parent glass at appropriate temperatures, where different calcium phosphate crystalline phases are grown in the parent glass samples during the heat treatment. The amounts of elements a...
متن کاملCharacterization of Thick and Thin Film SiCN for Pressure Sensing at High Temperatures
Pressure measurement in high temperature environments is important in many applications to provide valuable information for performance studies. Information on pressure patterns is highly desirable for improving performance, condition monitoring and accurate prediction of the remaining life of systems that operate in extremely high temperature environments, such as gas turbine engines. A number...
متن کاملSynthesis and characterization of Alumina (Al2O3) nanoparticles prepared by simple sol-gel method
Alumina is one of the most widely used ceramic materials as catalysts, catalyst supports and absorbents, and also wear resistant coating. This study focused on fabricating and characterizing of alumina ceramic nanoparticles fabricated using new and simple sol-gel method. Aluminium oxide (Al2O3) nanoparticles were synthesized by iron (III) nitrate 9-hydrate as precursor. Physicochemical properti...
متن کامل